Synthesis of magnetite nanoparticles under standing ultrasonication

Naoya Enomoto, Kosuke Yamada, Feng Dang, Miki Inada, Junichi Hojo

研究成果: ジャーナルへの寄稿学術誌査読

2 被引用数 (Scopus)


Magnetite nanoparticles were synthesized by oxidizing a Fe(OH)2 precipitate in various ultrasonic (US) fields including traveling wave (TW; 20 kHz) driven by a horn-type homogenizer and standing waves (SW; 45,100, 200 kHz) driven by a cleaner-type sonicator. Compared to a process with mechanical stirring (MS), each of US treatment completed the magnetite formation in much shorter time. The size of the nanoparticles decreased with the decreasing initial [Fe2+] concentration. Noticeably at [Fe2+] = 0.001 mol/L, no more particles but brown amorphous sols were formed in either MS or TW process. To the contrary, black magnetite nanoparticles were formed in the SW process as usual as higher concentration. The SW ultrasonication enabled to gather cavitation bubbles in its nodes, and then it is inferred that high supersaturation enough to form nanoparticles were achieved locally in the nodes of the SW field.

ジャーナルFuntai Oyobi Fummatsu Yakin/Journal of the Japan Society of Powder and Powder Metallurgy
出版ステータス出版済み - 4月 2009

!!!All Science Journal Classification (ASJC) codes

  • 機械工学
  • 産業および生産工学
  • 金属および合金
  • 材料化学


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