Synthesis and Rietveld analysis for CoSb3 compounds prepared by Sb self-flux method

Takeshi Souma; Michitaka Ohtaki

doi:10.1109/ICT.2005.1519903

Synthesis and Rietveld analysis for CoSb₃ compounds prepared by Sb self-flux method

Takeshi Souma, Michitaka Ohtaki

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution

2 Citations (Scopus)

Abstract

High purity CoSb₃ bulk crystals have been successfully synthesized by Sb self-flux method and a relation between reaction conditions and chemical composition on the method has been systematically analyzed by powder XRD study using the Rietveld analysis. Sb self flux method at 923 K using 100 mesh Co elements can directly provide a single phase CoSb₃ bulk crystal in a brief time of 10 h. Advantages of Sb self-flux methods will be discussed compared with other preparation methods.

Original language	English
Title of host publication	Proceedings - ICT'05
Subtitle of host publication	24th International Conference on Thermoelectrics
Pages	121-124
Number of pages	4
DOIs	https://doi.org/10.1109/ICT.2005.1519903
Publication status	Published - 2005
Event	ICT'05: 24th International Conference on Thermoelectrics - Clemson, SC, United States Duration: Jun 19 2005 → Jun 23 2005

Publication series

Name	International Conference on Thermoelectrics, ICT, Proceedings
Volume	2005

Other

Other	ICT'05: 24th International Conference on Thermoelectrics
Country/Territory	United States
City	Clemson, SC
Period	6/19/05 → 6/23/05

All Science Journal Classification (ASJC) codes

Engineering(all)

Access to Document

10.1109/ICT.2005.1519903

Cite this

Synthesis and Rietveld analysis for CoSb₃ compounds prepared by Sb self-flux method. / Souma, Takeshi; Ohtaki, Michitaka.
Proceedings - ICT'05: 24th International Conference on Thermoelectrics. 2005. p. 121-124 1519903 (International Conference on Thermoelectrics, ICT, Proceedings; Vol. 2005).

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution

Souma, T & Ohtaki, M 2005, Synthesis and Rietveld analysis for CoSb₃ compounds prepared by Sb self-flux method. in Proceedings - ICT'05: 24th International Conference on Thermoelectrics., 1519903, International Conference on Thermoelectrics, ICT, Proceedings, vol. 2005, pp. 121-124, ICT'05: 24th International Conference on Thermoelectrics, Clemson, SC, United States, 6/19/05. https://doi.org/10.1109/ICT.2005.1519903

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