TY - JOUR
T1 - Lithium niobium disulfide, Li0.63NbS2
AU - Salyer, Pamela A.
AU - Barker, Marten G.
AU - Blake, Alexander J.
AU - Gregory, Duncan H.
AU - Wilson, Claire
PY - 2003/1/1
Y1 - 2003/1/1
N2 - Lithium niobium disulfide, Li0.63NbS2, has been prepared by a metathesis reaction between physically separated solid reactants, i.e. separated reactant metathesis (SRM). Single-crystal data were collected at reduced temperature [150 (2) K], yielding a refined Li content of y = 0.63 (6). The Li content in the crystalline samples was also determined analytically by flame photometry. The compound crystallizes in hexagonal space group P63/mmc (No. 194), with Li+ ions situated in octahedral sites between NbS2 layers.
AB - Lithium niobium disulfide, Li0.63NbS2, has been prepared by a metathesis reaction between physically separated solid reactants, i.e. separated reactant metathesis (SRM). Single-crystal data were collected at reduced temperature [150 (2) K], yielding a refined Li content of y = 0.63 (6). The Li content in the crystalline samples was also determined analytically by flame photometry. The compound crystallizes in hexagonal space group P63/mmc (No. 194), with Li+ ions situated in octahedral sites between NbS2 layers.
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U2 - 10.1107/S0108270102021844
DO - 10.1107/S0108270102021844
M3 - Article
C2 - 12506209
AN - SCOPUS:0037258041
SN - 0108-2701
VL - 59
SP - i4-i6
JO - Acta Crystallographica Section C: Crystal Structure Communications
JF - Acta Crystallographica Section C: Crystal Structure Communications
IS - 1
ER -