Direct synthesis of Mg2FeH6 by mechanical alloying

J. Huot; S. Boily; E. Akiba; R. Schulz

doi:10.1016/S0925-8388(98)00725-7

Direct synthesis of Mg₂FeH₆ by mechanical alloying

J. Huot, S. Boily, E. Akiba, R. Schulz

Research output: Contribution to journal › Article › peer-review

120 Citations (Scopus)

Abstract

The hydride Mg₂FeH₆ was synthesized by high-energy ball milling of MgH₂ and Fe under argon atmosphere without subsequent sintering. After 60 h of milling, 56% wt. of Mg₂FeH₆ was synthesized. This yield was deduced from Rieltveld analysis of the X-ray powder measurements and confirmed by pressured differential scanning calorimeter (PDSC). Hydrogen capacity measurements indicated that the loss of capacity with cycling is minimal.

Original language	English
Pages (from-to)	306-309
Number of pages	4
Journal	Journal of Alloys and Compounds
Volume	280
Issue number	1-2
DOIs	https://doi.org/10.1016/S0925-8388(98)00725-7
Publication status	Published - Oct 23 1998
Externally published	Yes

All Science Journal Classification (ASJC) codes

Mechanics of Materials
Mechanical Engineering
Metals and Alloys
Materials Chemistry

Access to Document

10.1016/S0925-8388(98)00725-7

Cite this

@article{78efcaaf618247a7a2004da8ea260c4f,

title = "Direct synthesis of Mg2FeH6 by mechanical alloying",

abstract = "The hydride Mg2FeH6 was synthesized by high-energy ball milling of MgH2 and Fe under argon atmosphere without subsequent sintering. After 60 h of milling, 56% wt. of Mg2FeH6 was synthesized. This yield was deduced from Rieltveld analysis of the X-ray powder measurements and confirmed by pressured differential scanning calorimeter (PDSC). Hydrogen capacity measurements indicated that the loss of capacity with cycling is minimal.",

author = "J. Huot and S. Boily and E. Akiba and R. Schulz",

year = "1998",

month = oct,

day = "23",

doi = "10.1016/S0925-8388(98)00725-7",

language = "English",

volume = "280",

pages = "306--309",

journal = "Journal of Alloys and Compounds",

issn = "0925-8388",

publisher = "Elsevier BV",

number = "1-2",

}

TY - JOUR

T1 - Direct synthesis of Mg2FeH6 by mechanical alloying

AU - Huot, J.

AU - Boily, S.

AU - Akiba, E.

AU - Schulz, R.

PY - 1998/10/23

Y1 - 1998/10/23

N2 - The hydride Mg2FeH6 was synthesized by high-energy ball milling of MgH2 and Fe under argon atmosphere without subsequent sintering. After 60 h of milling, 56% wt. of Mg2FeH6 was synthesized. This yield was deduced from Rieltveld analysis of the X-ray powder measurements and confirmed by pressured differential scanning calorimeter (PDSC). Hydrogen capacity measurements indicated that the loss of capacity with cycling is minimal.

AB - The hydride Mg2FeH6 was synthesized by high-energy ball milling of MgH2 and Fe under argon atmosphere without subsequent sintering. After 60 h of milling, 56% wt. of Mg2FeH6 was synthesized. This yield was deduced from Rieltveld analysis of the X-ray powder measurements and confirmed by pressured differential scanning calorimeter (PDSC). Hydrogen capacity measurements indicated that the loss of capacity with cycling is minimal.

UR - http://www.scopus.com/inward/record.url?scp=0032180525&partnerID=8YFLogxK

UR - http://www.scopus.com/inward/citedby.url?scp=0032180525&partnerID=8YFLogxK

U2 - 10.1016/S0925-8388(98)00725-7

DO - 10.1016/S0925-8388(98)00725-7

M3 - Article

AN - SCOPUS:0032180525

SN - 0925-8388

VL - 280

SP - 306

EP - 309

JO - Journal of Alloys and Compounds

JF - Journal of Alloys and Compounds

IS - 1-2

ER -

Direct synthesis of Mg₂FeH₆ by mechanical alloying

Abstract

All Science Journal Classification (ASJC) codes

Access to Document

Other files and links

Fingerprint

Cite this