TY - JOUR
T1 - Development of automatic combinatorial system for synthesis of nanoparticles using microreactors
AU - Watanabe, Kosuke
AU - Orimoto, Yuuichi
AU - Yamashita, Kenichi
AU - Uehara, Masato
AU - Nakamura, Hiroyuki
AU - Furuya, Takeshi
AU - Maeda, Hideaki
PY - 2011
Y1 - 2011
N2 - In this study, automatic system for combinatorial synthesis of nanoparticles (NPs) was developed and optimization of reaction parameter for NPs synthesis was performed. Microreactor was employed for kinetic control constantly. Programmable equipments were employed for additional speed up and used a microreactor. Six reaction condition parameters were systematically combined to produce CdSe synthesis condition sets. Reaction conditions of 3404 experimental sets were synthesized and characterized in 1 month. As a result of some multivariate analyses using the numerous and complicated data, we found as follows: 1) neural network is an effective method to analyze data from combinatorial synthesis, 2) weighting evaluation method was effective to find the condition for balanced NP properties.
AB - In this study, automatic system for combinatorial synthesis of nanoparticles (NPs) was developed and optimization of reaction parameter for NPs synthesis was performed. Microreactor was employed for kinetic control constantly. Programmable equipments were employed for additional speed up and used a microreactor. Six reaction condition parameters were systematically combined to produce CdSe synthesis condition sets. Reaction conditions of 3404 experimental sets were synthesized and characterized in 1 month. As a result of some multivariate analyses using the numerous and complicated data, we found as follows: 1) neural network is an effective method to analyze data from combinatorial synthesis, 2) weighting evaluation method was effective to find the condition for balanced NP properties.
UR - http://www.scopus.com/inward/record.url?scp=84898956526&partnerID=8YFLogxK
UR - http://www.scopus.com/inward/citedby.url?scp=84898956526&partnerID=8YFLogxK
U2 - 10.1088/1757-899X/18/8/082010
DO - 10.1088/1757-899X/18/8/082010
M3 - Conference article
AN - SCOPUS:84898956526
SN - 1757-8981
VL - 18
JO - IOP Conference Series: Materials Science and Engineering
JF - IOP Conference Series: Materials Science and Engineering
IS - SYMPOSIUM 5
M1 - 082010
T2 - 3rd International Congress on Ceramics, ICC 2011
Y2 - 14 November 2010 through 18 November 2010
ER -