Deformation behavior of ultrafine grained iron

Setsuo Takaki, K. Kawasaki, Y. Futamura, Toshihiro Tsuchiyma

    Research output: Chapter in Book/Report/Conference proceedingConference contribution

    18 Citations (Scopus)


    Work hardening behavior and microstructure development during deformation by cold rolling were investigated in iron with different grain size. Grain refinement makes the introduction of dislocation easier. For instance, under the same deformation condition (5% reduction in thickness), dislocation density is the order of 10 14m -2 in a coarse grained material (mean grain size; 20μm), while it reaches 7×10 15m 2 in an ultrafine grained material (0.25μm). It is well known that the yield stress of metals is enlarged with an increase in dislocation density on the basis of the Bailey-Hirsch relationship. However, it should be noted that the ultrafine grained material never undergoes usual work hardening although the dislocation density is surely enhanced to around the order of 10 16m -2: 0.2% proof stress is almost constant at 1.4-1.5GPa regardless of the amount of deformation. The dislocation density of 10 16m -2 is thought to be the limit value which can be achieved by cold working of iron and the yield stress of iron with this dislocation density (ρ) is estimated at 1.1 GPa from the Bailey-Hirsch relationship; σ d [Pa] = 0.1×10 9 + 10 ρ 1/2. On the other hand, yield stress of iron is enhanced by grain refinement on the basis of the Hall-Petch relationship; σ gb [Pa] = 0.1×10 9 + 0.6×10 9 d -1/2 as to the grain size d [μm]. This equation indicates that the grain size of 0.35 μm gives the same yield stress as that estimated for the limit of dislocation strengthening (1.1 GPa). As a result, it was concluded that work hardening can not take place in ultrafine grained iron with the grain size less than 0.35 μm because dislocation strengthening can not exceed the initial yield stress obtained by grain refinement strengthening.

    Original languageEnglish
    Title of host publicationNanomaterials by Severe Plastic Deformation, NanoSPD3 - Proceedings of the 3rd International Conference on Nanomaterials by Severe Plastics Deformation
    Number of pages6
    Publication statusPublished - Dec 1 2006
    Event3rd International Conference on Nanomaterials by Severe Plastics Deformation, NanoSPD3 - Fukuoka, Japan
    Duration: Sept 22 2005Sept 26 2005

    Publication series

    NameMaterials Science Forum
    ISSN (Print)0255-5476


    Other3rd International Conference on Nanomaterials by Severe Plastics Deformation, NanoSPD3

    All Science Journal Classification (ASJC) codes

    • Materials Science(all)
    • Condensed Matter Physics
    • Mechanics of Materials
    • Mechanical Engineering


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