TY - JOUR
T1 - A novel wet polymeric precipitation synthesis method for monophasic β-TCP
AU - Grigoraviciute-Puroniene, I.
AU - Tsuru, K.
AU - Garskaite, E.
AU - Stankeviciute, Z.
AU - Beganskiene, A.
AU - Ishikawa, K.
AU - Kareiva, A.
N1 - Publisher Copyright:
© 2017 The Society of Powder Technology Japan
PY - 2017/9
Y1 - 2017/9
N2 - β-Tricalcium phosphate (β-Ca3(PO4)2, β-TCP) powders were synthesized using wet polymeric precipitation method for the first time to our best knowledge. The results of X-ray diffraction analysis showed the formation of almost single a Ca-deficient hydroxyapatite (CDHA) phase of a poor crystallinity already at room temperature. With continuously increasing the calcination temperature up to 800 °C the crystalline β-TCP was obtained as the main phase. It was demonstrated that infrared spectroscopy is very effective method to characterize the formation of β-Ca3(PO4)2. The SEM results showed that β-Ca3(PO4)2 solids were homogeneous having a small particle size distribution. The β-TCP powders consisted of spherical particles varying in size from 100 to 300 nm. Fabricated β-TCP specimens were placed to the bones of the rats and maintained for 1–2 months. The histological properties of these samples will be also investigated.
AB - β-Tricalcium phosphate (β-Ca3(PO4)2, β-TCP) powders were synthesized using wet polymeric precipitation method for the first time to our best knowledge. The results of X-ray diffraction analysis showed the formation of almost single a Ca-deficient hydroxyapatite (CDHA) phase of a poor crystallinity already at room temperature. With continuously increasing the calcination temperature up to 800 °C the crystalline β-TCP was obtained as the main phase. It was demonstrated that infrared spectroscopy is very effective method to characterize the formation of β-Ca3(PO4)2. The SEM results showed that β-Ca3(PO4)2 solids were homogeneous having a small particle size distribution. The β-TCP powders consisted of spherical particles varying in size from 100 to 300 nm. Fabricated β-TCP specimens were placed to the bones of the rats and maintained for 1–2 months. The histological properties of these samples will be also investigated.
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U2 - 10.1016/j.apt.2017.06.014
DO - 10.1016/j.apt.2017.06.014
M3 - Article
AN - SCOPUS:85021327004
SN - 0921-8831
VL - 28
SP - 2325
EP - 2331
JO - Advanced Powder Technology
JF - Advanced Powder Technology
IS - 9
ER -